Search results for "Pulsed waveform"

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Effect of Pulse Current Mode on Microstructure, Composition and Corrosion Performance of the Coatings Produced by Plasma Electrolytic Oxidation on AZ…

2019

Plasma electrolytic oxidation (PEO) coatings were grown on AZ31 Mg alloy in a silicate-based electrolyte containing KF using unipolar and bipolar (usual and soft-sparking) waveforms. The coatings were dual-layered consisting of MgO, MgF2 and Mg2SiO4 phases. Surface morphology of the coatings was a net-like (scaffold) containing a micro-pores network, micro-cracks and granules of oxide compounds. Deep pores were observed in the coating produced by unipolar and usual bipolar waveforms. The soft-sparking eliminated the deep pores and produced the lowest porosity in the coatings. It was found that the corrosion performance of the coatings evaluated using EIS in 3.5 wt. % NaCl solution is mostly…

Materials scienceplasma electrolytic oxidationAlloyOxideElectrolyteengineering.materialpulsed waveformsCorrosionchemistry.chemical_compoundCoatingmental disordersMaterials Chemistryaz31 mg alloyComposite materialPorositycorrosion resistancesilicatePulsed waveformSurfaces and InterfacesPlasma electrolytic oxidationMicrostructureSurfaces Coatings and FilmsSettore ING-IND/23 - Chimica Fisica Applicatachemistrylcsh:TA1-2040engineeringlcsh:Engineering (General). Civil engineering (General)Coatings
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Corrosion and wear resistance of coatings produced on AZ31 Mg alloy by plasma electrolytic oxidation in silicate-based K2TiF6 containing solution: Ef…

2022

Abstract In this research, plasma electrolytic oxidation coatings were prepared on AZ31 Mg alloy in a silicate-based solution containing K2TiF6 using bipolar and soft sparking waveforms with 10, 20, and 30% cathodic duty cycles. The coatings displayed a net-like surface morphology consisted of irregular micro-pores, micro-cracks, fused oxide particles, and a sintered structure. Due to the incorporation of TiO2 colloidal particles and the cathodic pulse repair effect, most of the micro-pores were sealed. Long-term corrosion performance of the coatings was investigated using electrochemical impedance spectroscopy during immersion in 3.5 wt.% NaCl solution up to 14 days. The coating grown by t…

AZ31 Mg alloyWear resistanceMaterials scienceAlloyPlasma electrolytic oxidationMetals and AlloysOxideCorrosion resistancePulsed waveformPlasma electrolytic oxidationengineering.materialCathodic protectionCorrosionDielectric spectroscopychemistry.chemical_compoundSettore ING-IND/23 - Chimica Fisica ApplicatachemistryCoatingMechanics of MaterialsengineeringComposite materialLayer (electronics)Dipotassium titanium hexafluoride
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